388 XXXI International Mineral Processing Congress 2024 Proceedings/Washington, DC/Sep 29–Oct 3
APPENDIX
Appendix A
APPENDIX B
Crystallization size calculation
Peak Position
(2 Theta) FWHM
Crystallite Size
D (nm)
D (nm)
Average
22.01519 4.52E-07 17,350,000 1,438,859.85
22.03664 1.52E-01 51.207
24.63862 0.15839 49.002
26.55039 0.10442 74.047
27.98931 0.32639 23.617
28.61096 0.15128 50.885
29.79704 0.20015 38.357
30.96417 0.24253 31.567
32.15274 0.18352 41.596
35.56514 0.20953 36.103
36.3675 0.2266 33.308
42.53276 2.03E-02 365.055
Sample Identification
Anode Material Cu
K-Alpha1 Wavelength 1.540598
K-Alpha2 Wavelength 1.544426
Ratio K-Alpha2/K-Alpha1 0.5
Divergence Slit Fixed
Monochromator Used NO
Generator Voltage 40
Tube Current 40
File Date And Time 22/8/2023 16:55
Unit Cell
H K L 0 0 0
Scan Axis Gonio
Scan Range 4.999999999
Scan Step Size 0.0065651
No. Of Points 17517
Scan Type CONTINUOUS
Phi 291.3
Time Per Step 178.245
Figure B.1 Raw plot data from XRD
APPENDIX
Appendix A
APPENDIX B
Crystallization size calculation
Peak Position
(2 Theta) FWHM
Crystallite Size
D (nm)
D (nm)
Average
22.01519 4.52E-07 17,350,000 1,438,859.85
22.03664 1.52E-01 51.207
24.63862 0.15839 49.002
26.55039 0.10442 74.047
27.98931 0.32639 23.617
28.61096 0.15128 50.885
29.79704 0.20015 38.357
30.96417 0.24253 31.567
32.15274 0.18352 41.596
35.56514 0.20953 36.103
36.3675 0.2266 33.308
42.53276 2.03E-02 365.055
Sample Identification
Anode Material Cu
K-Alpha1 Wavelength 1.540598
K-Alpha2 Wavelength 1.544426
Ratio K-Alpha2/K-Alpha1 0.5
Divergence Slit Fixed
Monochromator Used NO
Generator Voltage 40
Tube Current 40
File Date And Time 22/8/2023 16:55
Unit Cell
H K L 0 0 0
Scan Axis Gonio
Scan Range 4.999999999
Scan Step Size 0.0065651
No. Of Points 17517
Scan Type CONTINUOUS
Phi 291.3
Time Per Step 178.245
Figure B.1 Raw plot data from XRD